1 line
12 KiB
Plaintext
1 line
12 KiB
Plaintext
+-----------------------------------+
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+ ADVANCED EXPLOSIVES BY MILAMBER +
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+ AND BEAVER CLEAVER +
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+ PART I : PRIMARY EXPLOSIVES +
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+-----------------------------------+
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+ THANX TO J.C. FOR HIS HELP WITH +
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+ PRIMARY EXPLOSIVES!!! THANKS TO +
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+ DRAGON MASTER FOR VARIOUS RECIPES +
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+ ON EXPLOSIVES! +
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+-----------------------------------+
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+ AN UNDERGROUND LIBRARY FILE +
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+-----------------------------------+
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INTRODUCTION:
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-------------
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TO BEGIN, IT IS NECESSARY TO REMEMBER THAT SECONDARY EXPLOSIVES ARE DETONATED
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ONLY BY ANOTHER EXPLOSIVE. NAMELY, THE PRIMARY EXPLOSIVES. IN THIS FILE, WE
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WILL DISCUSS HOW TO MAKE THESE EXPLOSIVES. YOU WILL NOTE THAT IS MUCH MORE
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DANGEROUS TO PREPARE PRIMARY EXPLOSIVES. HOWEVER, THE EXPLOSIVES IN THIS FILE
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ARE SAFE TO MAKE AS LONG AS ONE IS CAREFUL, SO USE COMMON SENSE AND READ ALL
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OF THE DIRECTIONS A FEW TIMES BEFORE STARTING. DO NOT JUST START WITHOUT
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READING ALL OF THE CAUTIONS ON AN EXPLOSIVE!!!
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DDNP
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----
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DDNP IS A PRIMARY EXPLOSIVE USED IN THE FABRICATION OF DETONATORS. IT IS TO
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BE USED WITH A BOOSTER EXPLOSIVE SUCH AS PICRIC ACID OR RDX.
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MATERIALS:
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----------
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PICRIC ACID (SEE FILE #IV)
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FLOWERS OF SULFUR(DRUG STORE)
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LYE(DRUG STORE)
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SULFURIC ACID
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POTASSIUM OR SODIUM NITRITE
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WATER
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TWO HEAT RESISTANT GLASS CUPS
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STIRRING ROD
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SCALE
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PAPER TOWELS
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TEASPOON AND TABLESPOON
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EYEDROPPER
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HEAT SOURCE
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CONTAINERS
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TAPE
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PROCEDURE
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---------
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1. IN ONE OF THE GLASS CUPS, MIX 1/2 A GRAM OF LYE WITH TWO TABLESPOONS WARM
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WATER.
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2. DISSOLVE ONE TEASPOON OF PICRIC ACID IN THE WATER-LYE SOLUTION. STORE UNTIL
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STEP 5
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3. PLACE 1/4 OF A TEASPOON (1 ML) OF WATER IN THE OTHER GLASS CUP. ADD 1/2 A
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TEASPOON (2+1/2 GRAMS) OF SULFUR AND 1/3 OF A TEASPOON (2+1/2 G) OF LYE TO THE
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WATER.
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4. BOIL SOLUTION OVER HEAT SOURCE UNTIL COLOR TURNS DARK RED. REMOVE AND
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ALLOW TO COOL.
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5. IN THREE PORTIONS ADD THE SULFUR-LYE SOLUTION TO THE PICRIC ACID-LYE
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SOLUTION. STIR WHILE POURING. ALLOW MIXTURE TO COOL.
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6. FILTER MIXTURE THROUGH A PAPER TOWEL INTO A CONTAINER. SMALL RED PARTICLES
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WILL COLLECT ON THE PAPER. DISCARD THE LIQUID.
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7. DISSOLVE THE RED PARTICLES IN 1/4 OF A CUP BOILING WATER.
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8. SEE STEP 6.. EXCEPT DISCARD THE PARICLES LEFT ON THE PAPER -------
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9. USING AN EYEDROPPER SLOWLY ADD THE SULFURIC ACID TO THE FILTERED SOLUTION
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UNTIL IT TURNS ORANGE-BROWN.
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10. ADD 1/2 TEASPOON(2+1/2 G) MORE OF SULFURIC ACID TO THE SOLUTION. ALLOW TO COOL TO ROOM TEPM.
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11. IN A SEPARATE CONTAINER, DISOLVE 1/4 TEASPOON(1.8 G) OF SODIUM OR POTASSIUM NITRITE IN 1/3 CUP(80 ML.) OF WATER.
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12. ADD THIS SOLUTION IN ONE PORTION WHILE STIRRING TO THE ORANGE-BROWN SLOUTION. ALLOW THE MIXTURE TO STAND FOR 10 MINUTES. THE MIXTURE WILL TURN LIGHT BROWN.
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*****CAUTION: KEEP MIXTURE AWAY FROM FLAME. MIXTURE IS NOW A PRIMARY EXPLOSIVE*****
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LEAD PICRATE
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------------
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LEAD PICRATE IS USED AS A PRIMARY EXPLOSIVE IN THE FASHIONING OF DETONATORS.
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IT IS TO BE USERD WITH A BOOSTER EXPLOSIVE SUCH AS PICRIC ACID OR R.D.X.
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MATERIALS:
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----------
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LEAD MONOXIDE
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PICRIC ACID
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METHYL ALCOHOL
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DISH OR SAUCER (CHINA OR GLASS)
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TEASPOON
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IMPROVISED SCALE
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FLAT PAN
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CONTAINERS
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HEAT SOURCE(OPTIONAL)
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WATER(OPTIONAL)
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PROCEDURE
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---------
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1. WEIGH 2 GRAMS OF LEAD MONOXIDE AND PICRIC ACID. PLACE EACH IN A SEPERATE
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CONTAINER. MAKE SURE THAT THE CONTAINER THAT YOU PLACE THE PICRIC ACID IN IS
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, IF IT IS METAL, TIN OR ALUMINUM.
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2. PLACE 2 TEASPOONS (10 ML) OF ALCOHOL IN A DISH. ADD THE PICIRC ACID TO THE
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ALCOHOL AND STIR WITH A WOODEN OR PLASTIC ROD.
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3. ADD THE LEAD MONOXIDE TO THE MIXTURE WHILE STIRRING.
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** CAUTION AT THIS POINT THE SOLUTION IS A PRIMARY EXPLOSIVE - KEEP AWAY FROM
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HEAT AND FLAME!!!! **
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4. CONTINUE STIRRING THE MIXTURE UNTIL THE ALCOHOL HAS EVAPORATED. THE
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MIXTURE WILL SUDDENLY THICKEN.
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5. STIR MIXTURE OCCASIONALLY TO PREVENT LUMPS FROM FORMING UNTIL A POWDER HAS
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FORMED. A FEW LUMPS WILL REMAIN.
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** CAUTION, BE VERY CAREFUL OF DRY MATERIAL FORMING ON THE INSIDE OF THE
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CONTAINER **
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6. SPREAD THIS POWDERED MIXTURE (THE LEAD PICRATE) IN A FLAT PAN TO AIR DRY.
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NOTE:
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-----
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IF POSSIBLE DRY THE MIXTURE IN A HOT, NOT BOILING WATER BATH FOR TWO HOURS.
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** EXPLOSIVE IS SHOCK SENSITIVE WHEN DRY AND ONLY LESS SO WHEN WET **
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MERCURY FULMINATE
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-----------------
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MERCURY FULMINATE IS A PRIMARY EXPLOSIVE USED IN THE FABRICATION OF
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DETONATORS. IT IS TO BE USED WITH A BOOSTER EXPLOSIVE SUCH AS PICRIC ACID OR
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R.D.X.
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MATERIALS:
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NITRIC ACID
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MERCURY
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ETHYL ALCOHOL 90% PURE
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PAPER TOWELS
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TEASPOON MEASURE (ALUMINUM OR WAX COATED)
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HEAT SOURCE
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CLEAN WOODEN STICK
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CLEAN WATER
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GLASS CONTAINERS
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TAPE
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PROCEDURE:
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----------
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1. DILUTE 5 TEASPOONS OF NITRIC ACID WITH 2 AND 1/2 TEASPOONS OF CLEAN WATER
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IN A GLASS CONTAINER BY ADDING THE ACID TO THE WATER.
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2. DISSOLVE 1/8 TEASPOON OF MERCURY IN THE ACID WATER SOLUTION. DARK RED
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FUMES WILL FORM. DO NOT INHALE FUMES! NOTE: IT MAY BE NECESSARY TO ADD ONE
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DROP OF WATER, AT A TIME TO START THE REACTION.
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3. WARM 10 TEASPOONS OF ALCOHOL IN A CONTAINER UNTIL THE ALCOHOL FEELS WARM
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TO THE INSIDE OF THE WRIST.
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4. POUR THE METAL-ACID SOLUTION INTO THE WARM ALCOHOL. REACTION SHOULD START
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IN LESS THAN 5 MINUTES. DENSE WHITE FUMES WILL BE GIVEN OFF DURING THE
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REACTION. ALLOW 15 TO 20 MINUTES FOR RECTION TO FINISH. FULMINATE WILL SETTLE
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TO THE BOTTOM.
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** CAUTION THIS REACTION GENERATES LARGE QUANTITIES OF TOXIC FUMES. DO THIS
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STEP OUTDOORS. DO NOT INHALE FUMES **
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5. FILTER THE SOLUTION THROUGH THE PAPER TOWELS. CRYSTALS MAY STICK TO THE
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SIDE OF THE CONTAINER. WASH THEM DOWN WITH A SQUIRT OF WATER.
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6. WASH THE CRYSTALS WITH 6 TEASPOONS OF ETHYL ALCOHOL.
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** HANDLE DRY EXPLOSIVES WITH EXTREME CARE **
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TRANSPORT ONLY WHEN WET!!!!
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TETRAMINE COPPER ][ CHLORATE (TACC)
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------------------------------------
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THIS IS A PRIMARY EXPLOSIVE THAT CAN BE MADE FROM SODIUM CHLORATE, COPPER
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SULFATE AND AMMONIA. THIS EXPLOSIVE IS TO BE USED WITH A BOOSTER EXPLOSIVE
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SUCH AS PICRIC ACID OR RDX.
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MATERIALS:
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----------
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SODIUM CHLORATE - MEDICINE, WEEDKILLER, HARDWARE STORE
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COPPER ][ SULFATE - DRUG STORE
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AMMONIUM HYDROXIDE - HOUSEHOLD AMMONIUM SMELLING SALTS
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ALCOHOL - 95% PURE
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WAX, CLAY, PITCH, ETC.
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WATER BOTTLE-NARROW MOUTH
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BOTTLES : WIDE MOUTH; MASON JARS
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TUBING: RUBBER, STEEL, COPPER
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SCALE
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HEAT SOURCE
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PAPER TOWELS
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PAN
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TAPE
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CUP
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PROCEDURE:
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1. MEASURE 1/3 TEASPOON (2 AND 1/2 GRAMS) OF SODIUM CHLORATE INTO A WIDE
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MOUTHED BOTTLE. ADD TWO TEASPOONS OF ALCOHOL.
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2. PLACE THE WIDE MOUTHED BOTTLE IN A PAN OF HOT WATER. ADD 1 TEASPOON (4
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GRAMS) OF COPPER ][ SULFATE TO THE MIXTURE. HEAT FOR A PERIOD OF 30 MINUTES
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JUST UNDER THE BOILING POINT AND STIR OCCASIONALLY.
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** CAUTION: KEEP SOLUTION AWAY FROM FLAME ; NOTE: KEEP VOLUME CONSTANT BY
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ADDING ADDITIONAL ALCOHOL EVERY 10 MINUTES. **
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3. REMOVE SOLUTION FROM PAN AND ALLOW TO COOL. COLOR OF SOLUTION WILL CHANGE
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FROM BLUE TO LIGHT GREEN. FILTER SOLUTION THROUGH A PAPER TOWEL INTO ANOTHER
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WIDE-MOUTHED BOTTLE. STORE THIS SOLUTION UNTIL READY FOR STEP 6.
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4. ADD 1 CUP (250 ML) OF AMMONIA TO A NARROW MOUTHED BOTTLE.
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5. PLACE TUBING IN THE NECK OF THE BOTTLE SO THAT IT EXTENDS ABOUT 1 AND 1/2
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INCHES INTO THE BOTTLE. SEAL TUBING WITH WAX, PITCH ETC.
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6. PLACE THE FREE END OF THE TUBING INTO THE ALCOHOL-SULFATE SOLUTION FROM
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STEP 3. HEAT BOTTLE OF AMMONIA IN A PAN OF HOT WATER, BUT NOT BOILING, FOR
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APPX. TEN MINUTES.
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7. BUBBLE AMMONIA GAS THROUGH THE SULFATE-ALCOHOL SOLUTION UNTIL THE COLOR
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CHANGES FROM A DARK GREEN TO A LIGHT BLUE. BUBBLE FOR ANOTHER 10 MINUTES.
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** CAUTION: AT THIS POINT THE SOLUTION IS A PRIMARY EXPLOSIVE, KEEP AWAY
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FROM FLAME **
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8. REMOVE THE BOTTLE AND REDUCE IT TO ABOUT 1/3 OF ITS ORIGINAL VOLUME BY
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PLACING IT IN THE OPEN AIR, OR A MOVING STREAM OF AIR.
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** NOTE: POUR SOLUTION INTO A FLAT CONTAINER FOR FASTER EVAPORATION. **
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9. FILTER SOLUTION INTO OTHER WIDE MOUTHED BOTTLE TO COLLECT CRYSTALS. WASH
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CRYSTALS WITH ONE TEASPOON OF ALCOHOL AND SET ASIDE TO DRY. (APPX. 16 HOURS)
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** CAUTION: EXPLOSIVE IS SHOCK AND FLAME SENSITIVE, STORE IN A STABLE, CAPPED
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CONTAINER. **
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** DRYING TIME MAY BE REDUCED TO TWO HOURS IF A HOT, NOT BOILING (OR BLOW
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BLOW THYSELF UP) WATER BATH IS USED. **
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NITROGEN TRIIODINE
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------------------
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NITROGEN TRIIODINE IS A PRIMARY EXPLOSIVE THAT IS COMPLETELY SAFE WHEN WET.
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THE AVAILABILITY OF THE MATERIALS RECQUIRED HOWEVER, LIMITS THE PRODUCTION OF
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THIS EXPLOSIVE.
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MATERIALS:
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----------
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GLASS, BEAKER, ETC.
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AMMONIUM HYDROXIDE - HOUSHOLD SMELLING SALTS
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WATER
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IODINE - IMPROVISED, CHEMICAL SUPPLY
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SCALE
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PROCEDURE:
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----------
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1. WEIGH THE GLASS, OR BEAKER. RECORD THE NUMBER FOR FUTURE USE.
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2. ADD EQUAL AMOUNT OF AMMONIUM HYDROXIDE AND WATER TO THE GLASS. WEIGH THE
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SOLUTION, SUBTRACT WEIGHT OF GLASS, AND DIVIDE BY TWO. RECORD THIS NUMBER.
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3. ADD THE WEIGHT CALCULATED ABOVE, IN IODINE CRYSTALS TO THE SOLUTION.
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PRECIPITATE WILL FALL TO THE BOTTOM.
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** CAUTION: EXPLOSIVE IS HIGHLY SHOCK SENSITIVE WHEN DRY, TO THE POINT OF A
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FLY SETTING IT OFF!! **
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H.M.T.D.
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--------
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HMTD IS A PRIMARY EXPLOSIVE USED IN THE FABRICATION OF DETONATORS. IT CAN
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MADE FROM HEXAMETHYLENE TETRAMINE AND HYDORGEN PEROXIDE.
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MATERIALS:
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----------
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HEXAMETHYLENE TETRAMINE (SOLD IN DRUGSTORES UNDER THE NAME OF METHENAMINE.)
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HYDROGEN PEROXIDE
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CITRIC ACID - IN GROCERY STORES UNDER SOUR SALTS
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PAN
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BOTTLES OR GLASSES
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TEASPOON
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WATER
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TAPE
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PROCEDURE:
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----------
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1. MEASURE 9 TEASPOONS OF HYDROGEN PEROXIDE INTO A CONTAINER.
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2. IN THREE PORTIONS DISSOLVE TWO AND ONE HALF TEASPOONS OF CRUSHED
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HEXAMETHYLENE TETRAMINE IN THE PEROXIDE.
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3. KEEP THE SOLUTION COOL FOR 30 MINUTES BY PLACING CONTAINER INTO A PAN OF
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COLD WATER.
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4. IN 5 PORTIONS DISSOLVE 4 AND 1/2 TEASPOONS OF CRUSHED CITRIC ACID IN THE
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HEXAMETHYLENE TETRAMINE SOLUTION.
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5. PERMIT SOLUTION TO STAND AT ROOM TEMPERATURE WHILE SOLID PARTICLES COLLECT
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ON THE BOTTOM OF THE CONTAINER.
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** NOTE: COMPLETE PRECIPITATION WILL TAKE PLACE IN 8-24 HOURS. **
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** CAUTION, AT THIS POINT THE MIXTURE IS A PRIMARY EXPLOSIVE, KEEP AWAY FROM
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HEAT AND FLAME **
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6. FILTER SOULTION THROUGH A PAPER TOWEL TO COLLECT SOLID PARTICLES.
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7. WASH PARTICLES WITH 6 TEASPOONS OF WATER BY POURING THE WATER OVER THEM.
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8. PLACE EXPLOSIVE PARTICLES INTO COMTAINER AND OLLOW TO DRY.
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** CAUTION: HANDLE DRY EXPLOSIVE WITH GREAT CARE, DO NOT SCRAPE OR HANDLE IT
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ROUGHLY, KEEP AWAY FROM SPARKS AND FLAMES. STORE IN A COOL DRY PLACE **
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SOME OF THE FOLLOWING MAY NOT BE PRODUCED DUE TO UNAVAILABILITY OF NECESSARY
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CHEMICALS. I WILL TRY TO HAVE A FORMULA FOR PRODUCTION OF THE NECESSARY
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CHEMICALS IN ABOUT 1-3 MONTHS.
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LEAD AZIDE
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---- -----
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RATE OF DETONATION:4500 M/SEC.
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THIS IS SENSITIVE CRYSTALS LIKE
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MERCURY FULMINATE, BUT EASIER TO MAKE. AND SAFER. IT IS USED IN DETONATERS
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AND CAN BE STORED FOR 15 MONTHS AT UP TO 80 DEGREES WITHOUT DECOMPOSITION.
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IT IS MADE BY SLOW ADDITION OF DILUTE SODIUM AZIDE TO DILUTE LEAD ACETATE
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OR LEAD NITRATE WITH CONSTANT STIRRING. RAPID MIXING OF MORE CONCENTRATED
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SOLTUTIONS MAKES AMORPHOUS AZIDE, WHICH IS MORE STABLE. DEXTRINATED LEAD AZIDE
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IS MADE BY ADDING A SOLUTION OF SODIUM AZIDE CONTAINING A LITTLE SODIUM
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HYDROXIDE TO A SOLUTION OF LEAD NITRATE
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OR ACETATE AND DEXTRIN. THE PRECIPITATE LEAD AZIDE IS WASHED WITH WATER AND
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STORED LIKE MERCURY FULMINATE. IT SHOULD CONTAIN AT LEAST 20% WATER WHEN
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STORED.
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LEAD STYPHNATE
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---- ---------
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LESS SENSITIVE THAN MERCURY FULMINATE OR LEAD AZIDE(WHICH ARE SENSITIVE TO
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EVERYTHING), BUT MORE SENSITIVE TO HEAT. BASIC LS IS MADE BY MIXING SOLTIONS
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OF LEAD ACETATE AND SODIUM OR MAGNESIUM STYPHNATE. THIS IS PRETTY USELESS,
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BUT CAN BE MADE INTO A SALT BY
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TREATMENT WITH DILUTE NITRIC ACID OR BY TREATING A SOLUTION OF LEAD NITRATE
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WITH SODIUM STYPHNATE IN THE PRESENCE OF ACETIC ACID. THIS IS USED IN BLASTING
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CAPS. IT CAN BE STORED UNDER WATER OR MIX OF WATER & ALCOHOL.
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+------------------------------------+
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+ CALL THESE TOXIC BOARDS: +
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||
+ THE MOB 313-782-9519 +
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+ D.A. ][ 313-271-1095 +
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||
+ D.A. MAIN 313-386-5469 +
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||
+ THE HOLE IN THE WALL 313-383-4996+
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||
+ MARBLE MADNESS 619-353-0970 +
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+------------------------------------+
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(C) JANUARY 1987, MILAMBER AND BEAVER.
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Downloaded from P-80 Systems......
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