80 lines
3.6 KiB
Plaintext
80 lines
3.6 KiB
Plaintext
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KNOCK-OUT DROPS
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Cloral Hydrate (Knock-out Drops)
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Chemicals: Equiptment:
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Bleach Distilling Set (see below)
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Sani-Flush Clorine Bottle
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Ethyl Alcohol Glass Tubing
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Sulfuric Acid Rubber Tubing
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Calcium Oxide Aquarium Aerator
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Basting Syringe
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Cooking Thermometer
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600 ml Beaker
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Water Glass
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______ _______
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/ \_/ \___
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_/ ||| \ Bucket of ice water
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/--|_| / | \ | \ | ____________/
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/ / o \ | \ |
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Bleach |_____| |________\___| To outside
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& \ _________ /
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Saniflush | \__/
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600 ml | |
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w/ aerator |__| __Collection
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Glass
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A piece of glass is fitted into the bottom of the stopper for the flask. To
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that is placed an eight-inch length of rubber tubing and at the end of this is
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the aerator. Two more pieces of glass is put in the top of the stopper.
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First, you will need pure alcohol so buy some 100
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proof vodka and distill it until you have about 12 oz.
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Put the alcohol in the flask.Put about two inches of bleach and A teaspoon of
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Sani-Flush in the chlorine bottle. This will generate the clorine gas that you
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will need. Start the clorine through the alcohol while the flask is still
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cold.
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Watch it carefully to see when the alcohol stops absorbing the clorine. Then
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light a alcohol lamp and place it under the 600 ml flask. Keep the flame low
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until the alcohol stops absorbing again. Raise the flame and repeat. Continue
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this untill the alcohol is boiling. Some of the alcohol will distill off into
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the collection bottle. Several times during the process, pour this back into
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the 600 ml beaker.
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When the alcohol is totally chlorinated the flask is poured into a
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porcelain dish and allowed to cool. If you have done this right the
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cooled product should be a crystaline mass of unrefined Cloral Hydrate.
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Now, pour strong sulfuric acid, three times the volume of the
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Cloral Hydrate, into the pan. Place this pan on your stove over gentle
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heat. When the cloral hydrate is melted, it and the sulfuric acid are
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stirred throughly pour this into the flask and heat again. But this
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time use the thermometer and don't let it get over 200 F.
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As the mixture heats up, the still impure cloral hydrate will rise
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to the surface. When it stops rising, use the basting syringe and draw
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the top off of the sulfuric acid. Repeat this until the pan is empty.
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Put the cloral hydrate (you drew it off in the last step) into the
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beaker and heat at about 190 F. for 20 minutes. This will get rid of
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any alcohol or acid still in it. Pour this back into the flask and add
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an equal amount of sulfuric acid. Swirl this around to mix it.
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Once again you must distill the mixture. But this time it is easy
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since the cloral hydrate will boil at 210 F and the sulfuric acid boils
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at 722 F. When finished pour out the acid, then wash and dry the flask.
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Now, put the powered Calcium Oxide, equal in volume to the cloral
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hydrate into the flask, add the cloral hydrate and distill again. Stop
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as soon as the surface of the oxide is dry.
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To use, add one part water to two parts { by volume } of the
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finished product. The dose is 1/28th of an oz ( 1 gram ). The best way
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to use this is to put it into a mixed drink, because it has abitter
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taste. In about 15 minutes, whoever you gave it to is out for the night.
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eof
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